Synthesis of Sn-doped ZnO hierarchical particles and their gas-sensing properties
- Author(s): Xi Qin 1 ; Xu Wang 1 ; Dawei Gu 1 ; Linjiang Shen 1
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View affiliations
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Affiliations:
1:
School of Physical and Mathematical Sciences , Nanjing Tech University , Nanjing, 211800 People's Republic of China
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Affiliations:
1:
School of Physical and Mathematical Sciences , Nanjing Tech University , Nanjing, 211800 People's Republic of China
- Source:
Volume 13, Issue 12,
December
2018,
p.
1638 – 1641
DOI: 10.1049/mnl.2018.5330 , Online ISSN 1750-0443
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In this work, un-doped and Sn-doped hierarchical ZnO particles with high dispersity were successfully fabricated by a facile liquid reaction. The prepared samples are characterised by X-ray diffraction and scanning electron microscopy. The as-synthesised hierarchical ZnO particles with a diameter of ∼1.5 μm were obtained by considerably intersecting thin nanosheets of ∼20 nm thickness. The morphology of ZnO structures can be varied by adjusting reaction parameters, e.g. reaction temperature, calcination temperature, and dopant concentration. On the basis of experimental results, the gas-sensing measurement displays that the sensor based on Sn-doped ZnO microstructures have a low detection of 10 ppm ethanol at an operational temperature of 250°C, demonstrating its outstanding gas-sensing performance. Therefore, the flower-like Sn-doped ZnO have prospective applications in a multifunction ethanol sensor. Moreover, the fabrication method reported in the work is facile, flexible and operable, it is possible to extend to synthesise other types of metal oxide-based applications in various fields.
Inspec keywords: II-VI semiconductors; calcination; nanosensors; nanoparticles; tin; nanofabrication; X-ray diffraction; wide band gap semiconductors; gas sensors; scanning electron microscopy; semiconductor growth; organic compounds; crystal microstructure; doping profiles; zinc compounds
Other keywords: calcination temperature; gas-sensing measurement; high dispersity; temperature 250.0 degC; ZnO structure morphology; reaction temperature; dopant concentration; operational temperature; X-ray diffraction; scanning electron microscopy; Sn-doped ZnO microstructures; nanosheets; reaction parameters; Sn-doped ZnO hierarchical particles; gas-sensing properties; ZnO:Sn; multifunction ethanol sensor; facile liquid reaction
Subjects: Semiconductor doping; Microstructure; Chemical sensors; Other methods of nanofabrication; Nanometre-scale semiconductor fabrication technology; Low-dimensional structures: growth, structure and nonelectronic properties; Microsensors and nanosensors; II-VI and III-V semiconductors; Chemical sensors; Other heat and thermomechanical treatments; Impurity concentration, distribution, and gradients; Structure of solid clusters, nanoparticles, nanotubes and nanostructured materials
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