access icon free Characterisation and investigation of antibacterial properties of nylon 66/TPS/Ag NPs nanofibre membranes

Electrospinning method was used to prepare nylon 66 nanofibre membranes in solution mixed with chloroform/formic acid. These nanofibres were covered with (3-mercaptopropyl) trimethoxysilane (TPS) that has a sulphur group, making it a suitable host for Ag nanoparticles (Ag NPs). Spraying of the as-prepared nylon 66/TPS surface first with silver nitrate solution and then scattering with a mixture of N2H4/NaBH4 used as reducing agents during the second process provides nanofibres with nylon 66/TPS/Ag NPs structure. Characterisation of the formed nanofibres was studied by Fourier transform infrared, scanning electron microscopy, X-ray diffraction and transmission electron microscopy techniques. The non-woven polyurethane coated with activated carbon particles and polyethylene mesh was utilised as the substrate and protective layers of as-prepared nanofibres, respectively. Finally, the antibacterial activity of nanofibre membranes against gram-positive and gram-negative bacteria was investigated by using the disk diffusion method and it was shown that the newly synthesised nanofibres presented very good antibacterial activity against the tested bacteria. The results of this study can be used for industrial applications such as antibacterial wound dressings or/and water disinfection filters.

Inspec keywords: nanoparticles; X-ray diffraction; scanning electron microscopy; antibacterial activity; microorganisms; Fourier transform infrared spectroscopy; membranes; electrospinning; nanofibres; chemical engineering; transmission electron microscopy

Other keywords: nylon 66 nanofibre membranes; chloroform/formic acid; water disinfection filters; transmission electron microscopy techniques; Fourier transform infrared; X-ray diffraction; scanning electron microscopy; transmission electron microscopy; electrospinning method; antibacterial properties; silver nitrate solution

Subjects: Engineering materials; Industrial processes

References

    1. 1)
    2. 2)
    3. 3)
    4. 4)
    5. 5)
    6. 6)
    7. 7)
    8. 8)
      • 13. Bicerano, J.: ‘Prediction of polymer properties’ (Marcel Dekker, New York, NY, 2002).
    9. 9)
    10. 10)
      • 36. Mehrabanian, M., Nasr-Esfahani, M.: ‘HA/nylon 6,6 porous scaffolds fabricated by salt-leaching/solvent casting technique: effect of nano-sized filler content on scaffold properties’, Int. J. Nanomed., 2011, 6, pp. 16511659.
    11. 11)
    12. 12)
    13. 13)
      • 27. Hyeung, P.J., Rezaul, K.M., Kyo, K.I., et al: ‘Electrospinning fabrication and characterization of poly(vinyl alcohol)/montmorillonite/silver hybrid nanofibers for antibacterial applications’, Colloid. Polym. Sci., 2009, 288, (1), pp. 115121.
    14. 14)
    15. 15)
    16. 16)
    17. 17)
      • 24. Sedaghat, S., Nasseri, A.: ‘Synthesis and stabilization of Ag nanoparticles on a polyamide (nylon 6, 6) surface and its antibacterial effects’, Int. Nano Lett., 2011, 1, (1), p. 22.
    18. 18)
    19. 19)
    20. 20)
    21. 21)
    22. 22)
    23. 23)
    24. 24)
    25. 25)
    26. 26)
    27. 27)
    28. 28)
    29. 29)
    30. 30)
    31. 31)
    32. 32)
      • 34. Charles, J., Ramkumaar, G.R., Azhagiri, S., et al: ‘FTIR and thermal studies on nylon-66 and 30% glass fibre reinforced nylon-66’, J. Chem., 2009, 6, (1), pp. 2333.
    33. 33)
    34. 34)
    35. 35)
    36. 36)
    37. 37)
    38. 38)
http://iet.metastore.ingenta.com/content/journals/10.1049/mnl.2018.5142
Loading

Related content

content/journals/10.1049/mnl.2018.5142
pub_keyword,iet_inspecKeyword,pub_concept
6
6
Loading