access icon free Hydrothermal synthesis and controlled growth of tungsten disulphide nanostructures from one-dimension to three-dimensions

Three kinds of tungsten disulphide (WS2) such as nanospheres, nanowires and nanobelts have been synthesised using cetyltrimethyl ammonium bromide (CTAB) as a surfactant. The structural features of the as-prepared WS2 were characterised by X-ray powder diffraction and scanning electron microscopy. The CTAB surfactants played a critical role in producing different WS2 nanostructures. The growth mechanism of WS2 nanostructures is proposed in detail and the schematic representation of the formation mechanism is also shown. Also, the optical absorption property of the WS2 nanostructures was investigated. This reported work may be helpful to investigate structurally other metal chalcogenide materials with different morphologies.

Inspec keywords: X-ray diffraction; tungsten compounds; scanning electron microscopy; semiconductor growth; ultraviolet spectra; crystal growth from solution; nanowires; visible spectra; nanofabrication; nanobelts; semiconductor materials

Other keywords: nanospheres; metal chalcogenide materials; hydrothermal synthesis; X-ray powder diffraction; optical absorption property; nanowires; cetyltrimethyl ammonium bromide; CTAB surfactants; WS2; tungsten disulfide nanostructures; controlled nanostructure growth; scanning electron microscopy; nanobelts

Subjects: Visible and ultraviolet spectra of other nonmetals; Optical properties of other inorganic semiconductors and insulators (thin films, low-dimensional and nanoscale structures); Crystal growth; Other semiconductor materials; Nanofabrication using crystal growth techniques; Low-dimensional structures: growth, structure and nonelectronic properties; Nanometre-scale semiconductor fabrication technology; Crystal growth from solution; Structure of solid clusters, nanoparticles, nanotubes and nanostructured materials

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