Monitoring of crystallisation phenomena by ultrasound

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Monitoring of crystallisation phenomena by ultrasound

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Nucleation and crystal growth from solution have been monitored in real time using ultrasound. A stainless steel test cell was designed in which a small volume of hot saturated copper (II) sulphate solution cools and crystallises. The hardware and software developed could be modified for in-line crystallisation monitoring.

Inspec keywords: ultrasonic applications; crystal growth from solution; process monitoring; nucleation; crystallisation

Other keywords: crystal growth from solution; test cell; process control; nucleation; US applications; real-time monitoring; in-line crystallisation monitoring

Subjects: Engineering materials; Crystal growth; Measurement by acoustic techniques; Control equipment and processes in production engineering; Crystal growth from solution; Sonic and ultrasonic applications

References

    1. 1)
      • M. Giulietti , M.M. Seckler , S. Derenzo , J.V. Valarelli . Changes in copper sulfatecrystal habit during cooling crystallisation. J. Cryst. Growth , 1089 - 1093
    2. 2)
      • R.E. Challis , J.A. Harrison , A.K. Holmes , R.P. Cocker . A wide bandwidthspectrometer for rapid ultrasonic absorption measurements in liquids. J. Acoust. Soc. Am. , 2 , 730 - 740
    3. 3)
      • J.W. Mullin . (1993) Crystallisation.
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